Description

Part I: Chromatography
- Introduction. Interests and specificities of the two familly of chromatography (gas and liquid). Transport mode, separation modes and dispersion effects.
- Instrumentation of the two chromatographic modes. Injection, evolution of new stationary phases, dectection mode (FID, UV, MS)...
- Introduction to sample preparation for the application before analysis by chromatography.
- Application
Part II: Chromatography
- Introduction. Interests and specificities of mass spectrometry. Principle, m/z ration, isotopic profile...
- Instrumentation of a mass spectrometer. Source, analyzeur, dectector...
- Introduction to fragmentation and structural characterization.
- Application
 

Compétences visées

In the term of the lecture, the students should be able:
- To understand the principles used specifically in chromatography and mass spectrometry.
- To identify the difference between gas and liquid chromatography
- To understand the plate theory and the kinetic theory in chromatography.
- To explain the techniques and the problems that could occurred
- To know the role of the different part of a mass spectrometer (source, analyzer, detector)
- To understand the concept of fragmentation and structural characterization
 

Bibliographie

Principles of polymerization, Second edition, George ODIAN, Ed. John Wiley& Sons, 1970
Chromatography: Principles and Instrumentation, Mark F. Vitha, ed. Wiley, 2016
Mass Spectrometry, Jürgen H Gross, ed. Springer Link, 2017

 

MCC

Les épreuves indiquées respectent et appliquent le règlement de votre formation, disponible dans l'onglet Documents de la description de la formation.

Régime d'évaluation

ECI (Évaluation continue intégrale)

Coefficient

1.0

Évaluation initiale / Session principale - Épreuves